We enable science by offering product choice, services, process excellence and our people make it happen. If the sampler still does not initialize correctly, showing the same error message, the metering device should be disassembled and inspected (you can ask for help from an Agilent Customer support Representative). Home; Translate. We have not been able to perform the alignment process, even after resetting both the tower/tray. Oven temperature: Ambient +4 450 Ambient +5 350 . Agilent 7890 Gas Chromatograph Features: The combination of precise pneumatic and temperature control leads to extremely precise retention time reproducibility, which is the basis for all chromatographic measurement. Many check valve problems are the result of small particles interfering with the operation of the check valve. Crawford Scientific is the UK's premier supplier of chromatography products, training, consultancy, and technical services.. With our in-house expertise and independent status, we can offer you the products and services which are right for your instrumentation and applications without manufacturer bias. It is recommended that these issues be fully evaluated before moving to in-depth troubleshooting. If the fault light stays on, obtain Agilent service. Yes No Introduction Overview The Agilent SPS 4 autosampler, represents the state- of- the- art in autosampler design and is the latest generation of autosamplers from Agilent. cd ~walkup/vnmrsys/Automation ls trl cd auto_201*mmdd_01 (the latest directory from the last command) nano logfile This will open the log file. Agilent University. 8 Agilent SPS 3 Autosampler Users Guide Only Agilent-trained, Agilent-qualified, or Agilent-approved customer support representatives may open panels or covers that are retained by screws. You can get the firmware revision number from the ChemStation software readily. agilent 1260 autosampler manual Menu. Vital maintenance procedures and troubleshooting tips. Note: Licenses for Agilents software products are not transferable. Read Online Konrad Wolf: Chronist im Jahrhundert der Extreme (Die Andere Bibliothek, Band 416) Doc. Check the condition of the plunger and the plunger seal and replace if worn or damaged. If still failing, the Error LEDs on the autosampler connection panel on the front of the instrument will display a code. Open a Linux terminal and enter the following commands. Our expertise gives peace of mind, a speedy turnaround and minimal down-time for your laboratory equipment. A - From autosampler/injector. 1. B - To detector. 1 of 2. Use, duplication or disclosure of Software is subject to Agi- lent Technologies standard commercial license terms, and non-DOD Departments and Agencies of the U.S. Government will Agilent Thanks so much for all your helpful contributions. + $94.00 shipping. Download Book Add Comment Band 416), Konrad Wolf: Chronist im Jahrhundert LC Troubleshooting Series - Part 7: Autosamplers and Injectors Autosamplers and injection methods can be a source of trouble if they are not used correctly. HP/ Agilent Autosamplers. Agilent LC Rheodyne series Agilent Valves Stator Face Part No. The GC/MS hardware has been working fine and we were troubleshooting a tailing issue. Alignment of the Sample Probe on the Agilent PSD 120 Troubleshooting and Maintenance of Atomic Absorption Systems: Part 3 - Graphite Furnace AAS By Carlos Vargas > over 1 year ago. The autosamplers are controlled by the Agilent Instant Pilot (G4208A) or by This Information Applies To: Agilent 5000 Series ICP-OES (5100, 5110, 5800, 5900) Issue How to calibrate the ICP-OES ICP-OES calibration is a two-step + ICP-OES Troubleshooting. And this maintenance guide will help you keep your Agilent 1200 Series running at optimal performance and peak efficiency. Agilent SPS 4 Autosampler Initialization Sequence and Troubleshooting By Carlos Vargas > over 1 year ago. Furthermore, if the system is Obtain Agilent service. If you wish to Guidelines are provided with guidelines on how to prevent and/or address issues with your autosampler or injection process. Tailored and flexible service plans with 48 hour response time designed around multiple machined laboratories and covering all analytical instrumentation. The Agilent 7693A ALS (Automatic Liquid Sampler) provides reliable, fast, and precise injections for Agilent GC and GC/MS systems. The Fault Light Is On Probable cause The injector door is open. Note the error code and contact your Agilent Service Representative. Blue Line syringes are designed to support the higher productivity features of the Agilent 7693A automatic liquid sampler, while If the pressure drops drastically (more than a few bar due to simple reduction of capillary backpressure), then the blockage is after the column: Go to step 6 , and if it does not point to a solution, go through steps 2 to 5 also. Agilent offers two major lines of syringes for Agilent liquid autosamplers: Blue line and gold standard syringes. Agilent 7693 Autosampler. There are four LED lights. Condition. 10 Agilent 1260 Infinity Standard Autosampler User Manual 1 Introduction to the Autosampler Introduction to the Autosampler Introduction to the Autosampler Figure 1 Overview of the Autosampler The Agilent 1260 Infinity autosamplers are designed for use with other modules of the Agilent 1200 Infinity Series, 1200 Series and 1100 Series LC Page 1 Agilent InfinityLab LC Series 1260 Infinity II Preparative Autosampler User Manual Agilent Technologies; Page 2 (June 1987) or any equivalent agency regu- lation or contract clause. 1050 Manual injector 7125 0101-0607 0101-0624 1100 Manual injector 7725 5063-6502 0100-1859 1100 Autosampler 7750-020, 7750-030 0101-0921 0100-1851 1100 Switching valve Agilent LC Rheodyne Series Agilent Valves Stator Face Part No. Learn more about GC SYRINGES. The problem has been . $5,250.00. Firmware of the autosampler module needs to be close match to the other modules used in the instrument, that's important. Agilent 1200 Hplc Manual - pekingduk.blstr.co Inside this guide you'll find: Essential facts about Agilent supplies and accessories. 6 Agilent 1290 Infinity Autosampler User Manual Contents 6 Troubleshooting and Diagnostics 89 Overview of the Modules Indicators and Test Functions 90 Status Indicators 91 User Interfaces 93 Agilent Lab Advisor Software 94 7 Error Information 95 What are Error Messages 97 General Error Messages 98 Module Error Messages 104 8 WARNINGTo disconnect the autosampler from line power, unplug the power cord. 6 Agilent 1260 Infinity High Performance Autosampler User Manual Contents 6 Troubleshooting and Diagnostics 79 Overview of the Modules Indicators and Test Functions 80 Status Indicators 81 User Interfaces 83 Agilent Lab Advisor Software 84 7 Error Information 85 What are Error Messages 87 General Error Messages 88 Module Error The two modules are connected by a control cable and both are turned on by the autosampler module. Download File PDF Agilent 1200 Hplc Manual the Agilent 1200 Series modules. Note in this example it is: The various parameters and settings contained in the method are implemented immediately. For this use the 7RUTXH PDF. We're working on bringing an instrument back up that hasn't been used frequently. If the Autosampler stops without any error message, or after the mechanic problems mentioned above were solved, there are at least two possibilities. 1) Automation is paused. It can happen for different reasons. Just Resume automation, as described above. Suggested Actions Fix the leak in the external instrument before restarting the autosampler. Check external instruments for a shut-down condition. Check the degasser for an error condition. Refer to the Reference Manual for the Agilent 1100 Series degasser. 56 Troubleshooting and Test Functions Remote Timeout Remote Timeout We guaranteed our products with Warranty. Then we started having issues with the autosampler tower/tray. It provides for all 1200 Series LC the possibility of a first guided diagnostic for typical HPLC symptoms and a status report stored as Adobe Acrobat pdf or as a printable file to assist users evaluating the instrument state. solved by replacing the Autosampler fan and the instrument is perfectly Suggested actions 1. 2 Disconnect the USB cable and initialize the autosampler to ensure that it is in a working state. To do this, turn off the power switch, wait 10 seconds and then turn the power switch on. If the Agilent SPS 4 completes the initialization sequence with no error indicators, then this usually indicates that the autosampler is working fine. All the Agilent part numbers you need in one easy-to-use guide. Page 4 In This Book This manual contains information about the Agilent 1100 Series thermostatted autosamplers. Removal of such panels or covers can expose parts that involve the risk of electric shock or personal injury. United States. Agilent G1888 Headspace Sampler Service Manual Attachments Agilent G1888 Headspace Sampler Service Manual (41 MB) Updating, or lowering, the firmware in the module is possible for the computer-savvy user, downloads from Agilent. HPLC, UPLC & IC PRODUCTS. Santa Clara, CA 95051. and measure the torque for each axis. Troubleshooting and Test Functions 41 The thermostatted autosamplers built-in troubleshooting and test functions 41 Status Indicators 42 Error Messages 42 Status Indicators 43 Power Supply Indicator 44 Instrument Status Indicator 45 ALS Thermostat Error Messages 46 Solvent A is 0.1% trifluoroacetic acid in water, solvent B is 0.1% trifluoroacetic acid in acetonitrile, and the gradient runs from 2 to 40% B in 4 min. Oven ramps/plateaus: Supports 20 oven ramps with 21 plateaus. Agilent 5973 GCMS Training Manual Draft - 06/12/17 S.V. Showing 124 of 42 results. To clean pump check valves, remove the pump head and immerse the entire head into a laboratory ultrasonic cleaner. The Fault And The Run Lights Are On Probable causes The injector is mounted incorrectly on the mounting post. Sonicate for about 30 minutes using a standard cleaning solution. Our analytical equipments are refurbished, tested, and certified. This troubleshooting guide is meant to help you diagnose and repair autosampler problems. In general, autosampler problems can be divided into three categories. 1Intermittent lock-ups with or without vial in the gripper fingers with error messages Many times the sampler is being used very heavily. 5301 Stevens Creek Blvd. The LED pattern, where 1 is on and 0 is off, corresponds to an error code and description (Table 1). The same pump was used as in Figure 5, but now with a column (30 mm x 2.1 mm i.d. the autosampler, syringes that have become sticky or frozen so that the plunger movement is restricted, or a build-up of film on the surface of the sample turret in the tower. 2. Ensure that the injector door is closed. Part No. Location: 1238 Hach Hall method used, and with the last autosampler sequence used. The modular design allows this autosampler to grow with your lab. Assess the problem by checking the log file. Setting up the Autosampler with Agilent ChemStation 51 Main Screens of the Autosampler with Agilent Instant Pilot (G4208A) 61 5 Optimizing Performance 65 Reset your autosampler (switching it off and on). The Agilent 7683B series automatic liquid sampler raises the standard for gas chromatography (GC) system performance and reliability. Part No. If no physical or mechanical obstructions can be identified, turn the unit back on and allow it to attempt the reset procedure again. HP / Agilent HPLC. AGILENT HP G1364B Preparative Scale Fraction Collector 1100 Series HPLC. To begin, the most pronounced difference between an autosampler and a manual injector are the physical modules (pictured below in figure 1) that come with the Agilent 1220 HPLC. Troubleshooting Agilent.com Carlos Vargas Was this helpful? The power supply still uses some power, even if the power switch on the front panel is turned off. Figure 1 Overview of the Autosampler The Agilent 1260 Infinity autosampler is designed for use with other modules of the Agilent 1200 Infinity Series, 1200 Series and 1100 Series LC, or with other LC systems if adequate remote co ntrol inputs and outputs are available. 3. LC Troubleshooting Series - Part 7: Autosamplers and Injectors Headquarters | Other sites. Agilent 7694 AutoSampler Control Manual -17- 03-914947-47:3 In the Acquisition parameters tab, required fields like the Run Name, the Run ID and the Acquisition length must be filled in before starting an analysis. 2. 7 Troubleshooting Guide for the Sample Transport Assembly Poor alignment, seen during vial pickup and vial replacement and/or when the needle hits the gripper arm STEP 4: Check the tension of the belts. [1] Manual injectors require more user involvement by utilizing an injector port, lever, and a waste vial. If the Gripper open/closed torque is not in the range, proceed with STEP 5. Find the error message: hit F6 and type error Agilent SB-C18) in use, and gradient elution. If the autosampler fails to initialize: Turn off the power and move the probe by hand on along each axis and check if there are any physical mechanical obstructions. Mass spectrometry, chromatography, spectroscopy, software, dissolution, sample handling and vacuum technologies courses. 6 Troubleshooting and Diagnostics This chapter gives an overview about the troubleshooting and diagnostic features and the different user interfaces. Created by Jo Boden over 1 year ago AVS 4, and autosampler for manual sample introduction. The Agilent SPS 4 is a random access, single probe autosampler, providing front- end automation for several Agilent instruments. Correct as required. This next-generation Agilent automatic liquid sampler for the Agilent 7890A, 6890N, 6890 Plus and 6850 Series. ICP-OES Detector and Instrument Calibration. the Autosampler with Agilent Instant Pilot (G4208A) Below the main screens for the use of the autosampler are shown.4 Using the Module Main Screens of the Autosampler with Agilent Instant Pilot (G4208A) The Configure screen allows to configure Symbolic Name of module Volumes On Missing Vessel behaviour Plate configuration Flush- 6 Agilent 1260 Infinity Standard Autosampler User Manual Contents Troubleshooting 68 Troubleshooting Guide for the Sample Transport Assembly 70 Agilent Lab Advisor Software 77 7 Error Information 79 What are Error Messages 81 General Error Messages 82 Autosampler Error Messages 88 8 Maintenance 101
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